H-1 NMR Spectroscopy 24-Hour TurnaroundFront of Queue available

Rapid, High-Resolution Proton (¹H) NMR Analysis with 24-Hour Turnaround for routine samples

H-1 NMR (Proton NMR or 1H NMR) is the most widely used NMR technique for determining molecular structure and purity. Our state-of-the-art 500 MHz Bruker NMR spectrometer delivers high-resolution spectra for structure elucidation, compound identification, and quality control.

What is H-1 NMR Spectroscopy?

H-1 NMR (Proton Nuclear Magnetic Resonance) spectroscopy is an analytical technique that detects hydrogen atoms in organic compounds. It provides detailed information about:

  • Molecular structure - Identifies the arrangement of hydrogen atoms in your compound
  • Chemical environment - Shows how hydrogens are connected to other atoms
  • Compound purity - Detects impurities and confirms sample composition
  • Functional groups - Identifies specific molecular features like CH3, CH2, aromatic rings, etc.

Common Applications

Structure Determination

Confirm the structure of newly synthesized compounds or unknown materials

Purity Analysis

Assess sample purity and identify impurities or byproducts

Quality Control

Verify product consistency for pharmaceuticals, agrochemicals, and fine chemicals

Research Support

Provide data for publications, patents, and regulatory submissions

Our H-1 NMR Capabilities

  • 500 MHz Bruker NMR - State-of-the-art high-field instrumentation for superior resolution
  • 24-hour turnaround - Routine H-1 NMR analysis completed within one business day with front of queue available for a fee
  • Multiple solvents - CDCl3, DMSO-d6, D2O, CD3OD, and others upon request
  • Variable temperature - Analysis from Room temp to +80°C available (highest temperatures only for short experiments)
  • Quantitative analysis - Accurate concentration and purity measurements (see Quantitative NMR)
  • Expert interpretation - Spectral interpretation assistance and structural assignment available upon request
  • GLP compliance - SOP protocols for regulatory submissions

Sample Requirements

Typical Sample Amount

  • 1-5 mg for most organic compounds
  • More material may be needed for low-solubility samples
  • Contact us if you have limited sample availability

Sample Form

  • Solid, liquid, or oil (must be soluble in deuterated solvent)
  • Should be free of magnetic particles
  • Minimal water content preferred

Turnaround Time & Pricing

Standard Turnaround: 1 business day

Front of Queue: Front of Queue avaiable for 2x price of routine and we will immediately run it next (please note you would like "Front of Queue" on the order form)

Factors affecting acquisition time:

  • Molecular weight and complexity
  • Desired signal-to-noise ratio
  • Number of scans required

For pricing information, please visit our Pricing page or contact us. Pricing depends on sample complexity and turnaround requirements.

What You'll Receive

Standard Deliverables

  • H-1 NMR spectrum
  • Peak picking
  • Integration values
  • Coupling constants (upon request)
  • Raw data files (Please mark FID box on orderform)
  • PDF report

Optional Add-Ons

  • Variable temperature - Study fluxional processes
  • Quantitative H-1 - Precise ratios

For complete structural characterization, consider combining H-1 NMR with:

  • C-13 NMR - Carbon functional group determination
  • 2D NMR - COSY, HSQC, HMBC for complex structures
  • DEPT/APT - Distinguish CH, CH2, and CH3 groups
  • P-31 NMR - For phosphorus-containing compounds
  • F-19 NMR - For fluorinated compounds

Ready to Submit Your Sample?

Get started with our fast, reliable H-1 NMR analysis services

Submit a Sample View Pricing

Questions? Contact us or call (858) 793-6057

Why Choose NuMega for H-1 NMR Testing?

30+ Years Experience

Founded in 1993, we've been providing expert NMR analysis to researchers and industry for over three decades

State-of-the-Art Equipment

Two 500 MHz Bruker NMR spectrometers ensure high-quality spectra and minimal downtime

Expert Support

Our team of analytical chemists can help interpret your results and solve complex structural problems